METAL SOLUTIONS

EOS Titanium Ti64 Grade 5

Material Data Sheet

EOS Titanium Ti64 Grade 5

EOS Titanium Ti64 Grade 5 is a Ti6Al4V alloy, which is well-known for having excellent mechanical properties: low density with high strength and excellent corrosion resistance. The alloy has low weight compared to superalloys and steels and higher fatigue resistance compared to other lightweight alloys. EOS Titanium Ti64 Grade 5 is a titanium alloy powder intended for manufacturing parts on EOS metal systems with EOS DMLS processes.

Parts built with EOS Titanium Ti64 Grade 5 powder can be machined, shot-peened and polished in as manufactured and heat treated states. Due to the layerwise building method, the parts have a certain anisotropy. Heat treatment is recommended to reduce internal stresses and increase ductility.

EOS Titanium Ti64 Grade 5 powder can be used on the EOS M 290 with a 40 µm and 80 µm process and on the EOS M 400-4 with an 80 µm process.

MAIN CHARACTERISTICS

  • Low weight combined with high strength
  • Excellent corrosion resistance
  • High fatigue resistance compared to other lightweight alloys
  • The parts fulfill chemical requirements for Grade 5 alloy

Download Process Data Sheet (PDF)

TYPICAL APPLICATIONS

  • Aerospace components
  • Automotive components
  • Other industrial applications where low weight in combination with high strength are required

The EOS Quality Triangle

EOS uses an approach that is unique in the AM industry, taking each of the three central technical elements of the production process into account: the system, the material and the process. The data resulting from each combination is assigned a Technology Readiness Level (TRL) which makes the expected performance and production capability of the solution transparent.

EOS incorporates these TRLs into the following two categories:
 
  • Premium products (TRL 7-9): offer highly validated data, proven capability and reproducible part properties. 
  • Core products (TRL 3 and 5): enable early customer access to newest technology still under development and are therefore less mature with less data.

All of the data stated in this material data sheet is produced according to EOS Quality Management System and international standards
EOS 3D Printing Solutions Quality Triangle

POWDER PROPERTIES

EOS Titanium Ti64 Grade 5 powder is classified as Grade 5 titanium alloy according to ASTM B348. The chemical composition is in compliance with standards ISO5832-3, ASTM F1472, ASTM F2924, and ASTM F3302.

Powder Chemical Composition (wt.-%)

Element Min. Max.
Ti - -
Al 5.5 6.75
V 3.5 4.5
O 0.0 0.2
N 0.0 0.05
C 0.0 0.08
H 0.0 0.015
Fe 0.0 0.3
Y 0.0 0.005

Powder Particle Size

GENERIC PARTICLE SIZE DISTRIBUTION 20 - 80 μm

SEM micrograph of Titanium Ti64 Grade 5 powder

HEAT TREATMENT

Description

As manufactured microstructure for additively manufactured Ti64 consists of fully acicular alpha prime (α´) phase. Standard heat treatments for titanium do not necessarily produce desired microstructures due to this different starting microstructure. Heat treatment is recommended to relieve stresses and to increase ductility. Use of vacuum furnace is highly recommended to avoid the formation of alpha case on the surface of the parts.

Steps

120min (± 30 min) at 800 °C (±10 °C) measured from the part in vacuum (1.3 x 10-3 -1.3 x 10-5mbar) followed by slow cooling under vacuum or argon.
Material mechanical properties are relatively insensitive to changes in heating and cooling rates, but longer treatment times may result in decreased strength and increased elongation.
Parts heat treated according to the recommended heat treatment have a microstructure consisting of fine alpha + beta (α + β) phase.

Process Data Sheet

EOS Titanium Ti64 Grade 5 for EOS M 290 | 40 µm

EOS M 290 - 40 µm - TRL 7

Process Information Metal

This process product was developed specifically for the production of parts with high fatigue strength without the need for Hot Isostatic Pressing (HIP).

Main characteristics:

  • Robust production of parts in small series and series production
  • Improved fatigue strength compared to previous generation EOS Titanium Ti64 products
  • Possibility for shortened overall production time by avoiding HIP as post-process treatment step
System Setup EOS M 290
EOS Material set Ti64_Grade23_040_HiPerM291_100
Software Requirements

EOSPRINT 2.5 or newer

EOSYSTEM 2.8 or newer

Recoater Blade HSS (High Speed Steel)
Nozzle EOS Grid Nozzle
Inert gas Argon
Sieve 90 µm
Additional Information
Layer Thickness 40 µm
Volume Rate 6.2 mm³/s
Min. Wall Thickness approx. 0.4 mm

Chemical and Physical Properties of Parts

The chemical composition of parts is in compliance with standards ASTM F136, ASTMF3001, and ASTM F3302. Composition complies with EOS Titanium Ti64 Grade 23 powder.

The areal defect percentage was determined from cross-cuts of the built parts using optical microscope fitted with a camera and analysis software. The analysis was carried out for a sample area of 15 x 15 mm. The defects were detected and analyzed with an image capture/ analysis software with an automatic histogram based filtering procedure on monochrome images. The density of the built specimen was measured according to ISO3369

 

 

Microstructure of the Produced Parts

Defects Thickness Result Number of Samples
Average Defect Percentage 40 µm 0.01 % -
Density Thickness Result Number of Samples

Mechanical Properties

Mechanical Properties

Mechanical Properties Heat Treated

EN ISO 6892-1 Room Temperature Yield Strength [MPa] Tensile Strength [MPa] Elongation at Break A [%] Reduction of Area Z [%] Number of Samples
Vertical 1010 1080 15 25 - -
Horizontal 970 1080 14 25 - -

As manufactured microstructure for additively manufactured Ti64ELI consists of fully acicular alpha prime (α‘) phase.
Standard heat treatments for titanium do not necessarily produce desired microstructures due to this different starting microstructure.
Heat treatment is recommended to relieve stresses and to increase ductility. Use of vacuum furnace is highly recommended to avoid the formation of alpha case on the surface of the parts. 

Heat Treatment Description: 
120min (± 30 min) at 800 °C (± 10°C) measured from the part in vacuum (1.3x10-3-1.3x10-5 mbar) followed by cooling under vacuum or argon quenching.

Material mechanical properties are relatively insensitive to changes in heating and cooling rates, but longer treatment times may result in decreased strength and increased elongation.
Parts heat treated according to the recommended heat treatment have a microstructure consisting of fine alpha + beta (α + β) phase.

Fatigue

Heat Treated
Fatigue strength [MPa] 595

Fatigue strength at 1x10 million cycles in heat treated state Fatigue strength determines a stress level where specimen fails at a defined number of stress cycles [ISO 12107]. Fatigue strength was estimated statistically according to ISO 12107. Testing was done according to ASTM E466. Fatigue results typically show large deviations due to the nature of the fatigue process [ISO 12107].

Surface Roughness

Coefficient of Thermal Expansion

ASTM E228 Temperature
9*10-6/K 25 – 100 ºC
9.4*10-6/K 25 – 200 ºC
9.7*10-6/K 25 – 300 ºC
Process Data Sheet

EOS Titanium Ti64 Grade 5 for EOS M 290 | 80 µm

EOS M 290 - 80 µm - TRL 3

Process Information Metal

This process product is optimized for faster production of parts with properties according to ASTM F1472. For most demanding applications, Hot Isostatic Pressing (HIP) is recommended to optimize high cycle fatigue properties

Main Characteristics:

  • Parameter set for fast and cost efficient production of Ti64 parts in small series or serial production
  • 15 - 30 % faster than EOS Ti64 Speed (60 µm) parameter set
  • 50 % faster than EOS Ti64 Grade 5 HiPer (40 µm) parameter set
  • Material fulfills ASTM F2924 mechanical requirements in heat treated state. For fatigue critical applications, HIP is recommended as post-treatment.
System Setup EOS M 290
EOS Material set Ti64Grade23_080_CoreM291_100
Software Requirements

EOSPRINT 2.5 or newer

EOSYSTEM 2.8 or newer

Recoater Blade HSS (High Speed Steel)
Nozzle EOS Grid Nozzle
Inert gas Argon
Sieve 90 µm
Additional Information
Layer Thickness 80 µm
Volume Rate 12.0 mm³/s

Chemical and Physical Properties of Parts

The chemical composition of parts is in compliance with standards ASTM F136, ASTM F3001, and ASTM F3302. Composition complies with EOS Titanium Ti64 Grade 23 powder.

 

Microstructure of the Produced Parts

Defects Thickness Result Number of Samples
Average Defect Percentage 80 µm < 0.1 % -

Mechanical Properties

Mechanical Properties Heat Treated

EN ISO 6892-1 Room Temperature Yield Strength [MPa] Tensile Strength [MPa] Elongation at Break A [%] Reduction of Area Z [%] Number of Samples
Vertical 1020 1110 15 25 - -
Horizontal 1000 1100 15 25 - -

As manufactured microstructure for additively manufactured Ti64ELI consists of fully acicular alpha prime (α‘) phase.
Standard heat treatments for titanium do not necessarily produce desired microstructures due to this different starting microstructure.
Heat treatment is recommended to relieve stresses and to increase ductility. Use of vacuum furnace is highly recommended to avoid the formation of alpha case on the surface of the parts. 

Heat Treatment Description: 
120min (± 30 min) at 800 °C (± 10°C) measured from the part in vacuum (1.3x10-3-1.3x10-5 mbar) followed by cooling under vacuum or argon quenching.

Material mechanical properties are relatively insensitive to changes in heating and cooling rates, but longer treatment times may result in decreased strength and increased elongation.
Parts heat treated according to the recommended heat treatment have a microstructure consisting of fine alpha + beta (α + β) phase.

Elongation at break A and reduction of area Z in heat treated state: Mean values above the standard limit, some outliers below the limit.

Mechanical Properties HIP

EN ISO 6892-1 Room Temperature Yield Strength [MPa] Tensile Strength [MPa] Elongation at Break A [%] Reduction of Area Z [%] Number of Samples
Vertical 920 1020 16 25 - -
Horizontal 900 1010 16 25 - -

Hardness

Fatigue

HIP
Fatigue strength [MPa] 675

High cycle fatigue strength was estimated statistically according to ISO 12107. Testing was done according to ASTM E466 with run-out limit 107 cycles.

Surface roughness - Vertical

Value

9 µm

Unit

Ra

Process Data Sheet

EOS Titanium Ti64 Grade 5 for EOS M 300-4 | 40 µm

EOS M 300-4 - 40 µm - TRL 3

System Setup EOS M 300-4
EOS Material set Ti64Grade5_040_CoreM304
Software Requirements

EOSPRINT 2.13 or newer

EOSYSTEM 2.17 or newer

Recoater Blade HSS (High Speed Steel)
Inert gas Argon
Sieve 90 µm
Additional Information
Layer Thickness 40 µm
Volume Rate up to 4 x 6.2 mm³/s

Chemical and Physical Properties of Parts

The chemical composition of parts is in compliance with standards ISO5832-3, ASTM F1472, ASTM F2924, and ASTM F3302. Composition complies with EOS Titanium Ti64 Grade 5 powder.

Microstructure of the Produced Parts

Defects Thickness Result Number of Samples
Average Defect Percentage 40 µm < 0.1 % -

Mechanical Properties

Mechanical Properties Heat Treated

EN ISO 6892-1 Room Temperature Yield Strength [MPa] Tensile Strength [MPa] Elongation at Break A [%] Reduction of Area Z [%] Number of Samples
Vertical 1070 1150 12 25 - -
Horizontal 990 1100 14 25 - -

Surface Roughness

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