Process Data Sheet

EOS NickelAlloy IN738 for EOS M 290 | 40 µm

EOS M 290 - 40 µm - TRL 5

Process Information Metal

EOS NickelAlloy IN738 is susceptible to formation of macrocracks upon heat treatment, dependant on part geometry.

Following are recommendations to mitigate the risk of macrocrack formation:
(1) shot peening of parts prior to heat treatment; (2) a combined stress relieve and solution treatment plus HIP treatment using pre-pressurization.

System Setup EOS M 290
EOS Material set IN738_040_CoreM291
Required Software Plan EOS BUILD
Software Requirements

EOSPRINT 2.15 or newer

EOSYSTEM 2.19 or newer 

 

Recoater Blade HSS (High Speed Steel)
Nozzle EOS Grid Nozzle
Inert gas Argon
Sieve 63 µm
Additional Information
Layer Thickness 40 µm
Volume Rate 2.7 mm³/s
Min. Wall Thickness 0.4 mm
Typical Dimensional Change after HT [%] - 0.2 % after HIP and ageing %

Chemical and Physical Properties of Parts

Powder and built part compositions are based on AMS 5410C.

Microstructure of the Produced Parts

Defects Thickness Result Number of Samples
Average Defect Percentage 40 µm 0.05 % 5
Average Defect Percentage 40 µm 0.001 % -

Mechanical Properties

Mechanical Properties HIP + Heat-treated

EN ISO 6892-1 Room Temperature | 40 µm Yield Strength [MPa] Tensile Strength [MPa] Elongation at Break A [%] Reduction of Area Z [%] Modulus of elasticity [GPa] Number of Samples
Vertical 935 1295 9.2 9.1 - -
Horizontal 1005 1275 5.4 5.8 - -

The recommended post-processing route for EOS NickelAlloy IN738 includes shot-peening, hot isostatic pressing (HIP) and ageing.

Extra care is required in post-processing since certain geometries printed in EOS NickelAlloy IN738 may be susceptible to formation of macro-cracks upon heat treatment. Geometries with notches or sharp changes of cross-section are particularly vulnerable.

- Shot-peening is recommended to induce compressive residual stress on the surface of the component.
- HIP is recommended to perform the combined stress relief, solution treatment (sub-solvus) and densification steps into a single heat treatment step.
- Ageing is required for precipitation strengthening.

For further details, alternative options, and the recommended order of post-processing operations please refer to the Post-Processing Guide Application Note for EOS NickelAlloy IN738, which can be found on MyEOS.

Shot-peening: 
Use zirconia beads or steel shot as media, and a suitably high pressure, e.g. 4 bar or higher.
Use a suitable stand-off distance of approximately 5 cm and slow travel speed, keeping the angle of incidence roughly perpendicular to the surface of the workpiece. Ensure good coverage of all surfaces, with special focus on overhangs, notches, and changes of cross-section.

HIP:
1. Heat from room temperature to 600°C in 40 mins.​ Increase pressure to ~200 MPa.
2. Hold at 600°C and ~200 MPa for 60 minutes.
3. Heat to 1120°C in 15 minutes. Maintain pressure of 200 MPa.
4. Hold at 1120°C and ~200 MPa for 240 minutes.
5. Cool rapidly to below 300°C within 8 minutes.

Ageing:
1. Heat to 850°C in 60 minutes.
2. Hold at 850°C for 24 hours.
3. Cool from 850°C to <300°C in 20 minutes.

Mechanical Properties As Manufactured

EN ISO 6892-1 Room Temperature | 40 µm Yield Strength [MPa] Tensile Strength [MPa] Elongation at Break A [%] Reduction of Area Z [%] Modulus of elasticity [GPa] Number of Samples
Vertical 825 1200 21.3 22.7 - -
Horizontal 955 1305 18.9 20.8 - -

Mechanical Properties Heat Treated

EN ISO 6892-2 760°C | 40 µm Yield Strength [MPa] Tensile Strength [MPa] Elongation at Break A [%] Reduction of Area Z [%] Modulus of elasticity [GPa] Number of Samples
Vertical 730 975 15.3 20.2 - -
Horizontal 775 995 7.8 10.3 - -

Mechanical Properties Heat Treated

EN ISO 6892-2 816°C | 40 µm Yield Strength [MPa] Tensile Strength [MPa] Elongation at Break A [%] Reduction of Area Z [%] Modulus of elasticity [GPa] Number of Samples
Vertical 580 795 16.3 19.1 - -
Horizontal 570 815 9.5 11.3 - -

Mechanical Properties Heat Treated

EN ISO 6892-2 871°C | 40 µm Yield Strength [MPa] Tensile Strength [MPa] Elongation at Break A [%] Reduction of Area Z [%] Modulus of elasticity [GPa] Number of Samples
Vertical 465 655 19.5 23.7 - -
Horizontal 460 660 10.5 10.5 - -

Mechanical Properties Heat Treated

EN ISO 6892-2 954°C | 40 µm Yield Strength [MPa] Tensile Strength [MPa] Elongation at Break A [%] Reduction of Area Z [%] Modulus of elasticity [GPa] Number of Samples
Vertical 295 430 24.6 26.9 - -
Horizontal 295 415 11.1 13.5 - -

Hardness

EN ISO 6508 Heat Treated
Value 417
Unit HV10
EN ISO 6508 Heat Treated
Value 44
Unit HRC
EN ISO 6508 As Manufactured
Value 350
Unit HV10
EN ISO 6508 As Manufactured
Value 38
Unit HRC

Stress rupture performance

Surface roughness

Coefficient of Thermal Expansion

ASTM E228 Heat Treated Temperature
11.2*10-6/K 25 – 100 ºC
12.2*10-6/K 25 – 200 ºC
12.8*10-6/K 25 – 300 ºC
13.2*10-6/K 25 – 400 ºC
13.5*10-6/K 25 – 500 ºC
13.8*10-6/K 25 – 600 ºC
14.2*10-6/K 25 – 700 ºC
14.6*10-6/K 25 – 800 ºC
15.2*10-6/K 25 – 900 ºC
16.3*10-6/K 25 – 1000 ºC
ASTM E228 As Manufactured Temperature
11.2*10-6/K 25 – 100 ºC
12.4*10-6/K 25 – 200 ºC
13*10-6/K 25 – 300 ºC
13.4*10-6/K 25 – 400 ºC
13.7*10-6/K 25 – 500 ºC
13.2*10-6/K 25 – 600 ºC
13.1*10-6/K 25 – 700 ºC
13.4*10-6/K 25 – 800 ºC
14.2*10-6/K 25 – 900 ºC
15.4*10-6/K 25 – 1000 ºC
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