Process Data Sheet

EOS NickelAlloy IN738 for EOS M 400-4 | 40 µm

EOS M 400-4 - 40 µm - TRL 3

Process Information Metal

EOS NickelAlloy IN738 is susceptible to formation of macrocracks upon heat treatment, dependant on part geometry.

Following are recommendations to mitigate the risk of macrocrack formation:
(1) shot peening of parts prior to heat treatment; (2) a combined stress relieve and solution treatment plus HIP treatment using pre-pressurization.

System Setup EOS M 400-4
EOS Material set IN738_040_CoreM400-4
Required Software Plan EOS BUILD
Software Requirements

EOSPRINT 2.15 or newer
EOSYSTEM 2.19 or newer 

Recoater Blade HSS (High Speed Steel)
Nozzle Standard
Inert gas Argon
Sieve 63 µm
Additional Information
Layer Thickness 40 µm
Volume Rate 2.68 mm³/s
Min. Wall Thickness 0.4 mm
Typical Dimensional Change after HT [%] - 0.2 % after HIP and ageing %

Chemical and Physical Properties of Parts

Powder and built part compositions are based on AMS 5410C.

Microstructure of the Produced Parts

Defects Thickness Result Number of Samples
Average Defect Percentage 40 µm 0.05 % -
Average Defect Percentage 40 µm 0.002 % -

Mechanical Properties

Mechanical Properties HIP + Heat-treated

EN ISO 6892-1 Room Temperature | 40 µm Yield Strength [MPa] Tensile Strength [MPa] Elongation at Break A [%] Reduction of Area Z [%] Modulus of elasticity [GPa] Number of Samples
Vertical 917 1344 10.8 11.5 173 -
Horizontal 964 1270 6.9 7.4 197 -

The recommended post-processing route for EOS NickelAlloy IN738 includes shot-peening, hot isostatic pressing (HIP) and ageing.

Extra care is required in post-processing since certain geometries printed in EOS NickelAlloy IN738 may be susceptible to formation of macro-cracks upon heat treatment. Geometries with notches or sharp changes of cross-section are particularly vulnerable.

- Shot-peening is recommended to induce compressive residual stress on the surface of the component.
- HIP is recommended to perform the combined stress relief, solution treatment (sub-solvus) and densification steps into a single heat treatment step.
- Ageing is required for precipitation strengthening.

For further details, alternative options, and the recommended order of post-processing operations please refer to the Post-Processing Guide Application Note for EOS NickelAlloy IN738, which can be found on MyEOS.

Shot-peening: 
Use zirconia beads or steel shot as media, and a suitably high pressure, e.g. 4 bar or higher.
Use a suitable stand-off distance of approximately 5 cm and slow travel speed, keeping the angle of incidence roughly perpendicular to the surface of the workpiece. Ensure good coverage of all surfaces, with special focus on overhangs, notches, and changes of cross-section.

HIP:
1. Heat from room temperature to 600°C in 40 mins.​ Increase pressure to ~200 MPa.
2. Hold at 600°C and ~200 MPa for 60 minutes.
3. Heat to 1120°C in 15 minutes. Maintain pressure of 200 MPa.
4. Hold at 1120°C and ~200 MPa for 240 minutes.
5. Cool rapidly to below 300°C within 8 minutes.

Ageing:
1. Heat to 850°C in 60 minutes.
2. Hold at 850°C for 24 hours.
3. Cool from 850°C to <300°C in 20 minutes.

Mechanical Properties As Manufactured

EN ISO 6892-1 Room Temperature | 40 µm Yield Strength [MPa] Tensile Strength [MPa] Elongation at Break A [%] Reduction of Area Z [%] Modulus of elasticity [GPa] Number of Samples
Vertical 880 1237 19.1 20.7 - -
Horizontal 957 1310 20.3 22.6 - -

Mechanical Properties Heat Treated

EN ISO 6892-2 650°C | Yield Strength [MPa] Tensile Strength [MPa] Elongation at Break A [%] Reduction of Area Z [%] Modulus of elasticity [GPa] Number of Samples
Vertical 897 1223 18.2 24 - -
Horizontal 926 1250 14.5 20 - -

Mechanical Properties Heat Treated

EN ISO 6892-2 760°C | 40 µm Yield Strength [MPa] Tensile Strength [MPa] Elongation at Break A [%] Reduction of Area Z [%] Modulus of elasticity [GPa] Number of Samples
Vertical 724 979 17.7 24 - -
Horizontal 763 981 9.8 14 - -

Mechanical Properties Heat Treated

EN ISO 6892-2 816°C | 40 µm Yield Strength [MPa] Tensile Strength [MPa] Elongation at Break A [%] Reduction of Area Z [%] Modulus of elasticity [GPa] Number of Samples
Vertical 556 812 17.2 23 - -
Horizontal 580 817 8.3 10.5 - -

Mechanical Properties Heat Treated

EN ISO 6892-2 871°C | 40 µm Yield Strength [MPa] Tensile Strength [MPa] Elongation at Break A [%] Reduction of Area Z [%] Modulus of elasticity [GPa] Number of Samples
Vertical 459 660 16.1 25 - -
Horizontal 455 660 7.8 8 - -

Mechanical Properties Heat Treated

EN ISO 6892-2 954°C | 40 µm Yield Strength [MPa] Tensile Strength [MPa] Elongation at Break A [%] Reduction of Area Z [%] Modulus of elasticity [GPa] Number of Samples
Vertical 296 423 15.3 15.5 - -
Horizontal 292 414 11.3 14.5 - -

Hardness

EN ISO 6508 Heat Treated
Value 405
Unit HV10
EN ISO 6508 As Manufactured
Value 345
Unit HV10

Stress rupture performance

Surface roughness

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